The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis–gas chromatographic–mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.Four years after the publication of the book Pyrolysis: Gas Chromatography/Mass Spectrometry of Polymeric Materials, WSPC is offering a second, extended and revised edition of this book to interested readers.Key FeaturesAnalytical Pyrolysis–GC/MS proved to be a valuable hyphenated technique for the analysis and identification of synthetic organic polymeric materials, their additives and for the analysis of biopolymers. This technique allows the direct analysis of very small sample amounts (5–200 µg) without the need of time-consuming sample preparation or after a simple sample derivatization. Pyrolysis–GC/MS can be applied to research and development of new materials, quality control, characterization and competitor product evaluation, medicine, biology and biotechnology, geology, airspace, and environmental analysis to forensic purposes or conservation and restoration of cultural heritage. These applications cover analysis and identification of polymers/copolymers and additives in components of automobiles, tires, packaging materials, textile fibres, coatings, adhesives, half-finished products for electronics, paints, or varnishes, lacquers, leather, paper, or wood products, food, pharmaceuticals, surfactants, and fragrances. Pyrolysis–GC/MS allows the confirmation of the source of a failed product, the identification of contaminants causing failure, the competitive analysis, as well as overcoming a problem in product development or quality control. The obtained analytical results are then used for troubleshooting and remedial action of the technological processRenewable biopolymers from different natural sources have attracted much attention in the recent past years because of their use in different areas such as food, cosmetics, medicines, fuels and construction materials. Pyrolysis–GC/MS is highly suitable for practical studies of biopolymers. In recent years, this analytical technique has found wide application in environmental analysis to study the chemical composition and quantification of micro(nano)plastics

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